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Download e-book for iPad: Analytical Methods in Supramolecular Chemistry by Christoph A. Schalley

By Christoph A. Schalley

An summary of the concepts used to envision supramolecular aggregates from a methodological perspective. Edited via a emerging megastar locally and an skilled writer, it is a definitive survey of helpful sleek analytical equipment for knowing supramolecular chemistry, from NMR to single-molecule spectroscopy, from electron microscopy to extraction tools. A definitive learn of this box touching many interdisciplinary parts akin to molecular units, biology, bioorganic chemistry, fabric technological know-how, and nanotechnology.

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Dekker, New York, 2004, 1257. A. Klug, Angew. Chem. 1983, 95, 579; Angew. , Int. Ed. Engl. 1983, 22, 565. L. F. Lindoy, I. M. Atkinson, SelfAssembly in Supramolecular Chemistry, Royal Society of Chemistry, Cambridge 2000. For a review, see: F. Hof, S. L. Craig, C. Nuckolls, J. , Angew. Chem. 2002, 114, 1556; Angew. Chem. Int. Ed. 2002, 41, 1488. a) D. H. Busch, N. A. Stephensen, Coord. Chem. Rev. 1990, 100, 119; b) R. Cacciapaglia, L. Mandolini, Chem. Soc. Rev. 1993, 22, 221; c) N. V. Gerbeleu, V.

K. Y. Wong, Angew. Chem. 2001, 113, 1586; Angew. Chem. Int. Ed. 2001, 40, 1538; c) P. -M. -P. Sauvage, J. Am. Chem. Soc. 2003, 125, 2016. a) F. Diederich, J. Chem. Educ. 1990, 67, 813; b) P. Scrimin, P. Tecilla, U. Tonellato, J. Phys. Org. Chem. -M. Lehn, Appl. Catal. A, 1994, 113, 105; d) M. C. Feiters, in: Comprehensive Supramolecular Chemistry, Eds: J. L. Atwood, J. E. D. Davies, D. D. MacNicol, F. Vo¨gtle, Pergamon Press, Oxford 1996, Vol. 11, p. 267; e) J. K. M. Sanders, Chem. Eur. J. 1998, 4, 1378.

CŠ ¼ 1 d À dh Á ½HŠ0 Á a dc À dh ð2:54Þ If all constants (a, dh , dg and dc ) were obtainable, [C] would be determined from d and the experimental conditions ([H]0 ). Since dc cannot be obtained directly, a titration experiment and regression are necessary for the evaluation of complex concentration. 3 Data Treatment for NMR Method Rose–Drago Method for NMR Spectroscopy In this section, the way to apply the original Rose–Drago method for UV/vis spectroscopy to NMR titration data is described, especially for host–guest systems on fast exchange.

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